Experimental Study on Comprehensive Recovery of Gold, Silver, Copper, and Cobalt from Gold Containing Arsenic, Copper, and Cobalt Gold Concentrates

Abstract : A method for the comprehensive recovery of gold, silver, copper and cobalt from arsenic, copper and cobalt gold concentrates was developed. The process is a two-stage roasting process. Stage I roasting is decomposition roasting. As2O3 is volatilized and removed at 400-500 DEG C, and Stage II roasting is sulfation roasting. The second stage calcination was performed by adding the additive R2 to the calcine slag I at 600 to 650°C. The calcined slag was leached with hot water and 10% H2SO4 to make the cobalt enter the solution, and the gold and silver in the acid leaching slag were subjected to cyanogen. Refining with leaching. The tests showed that the gold leaching rate was 92.78%, the silver leaching rate was 47.06%, and the cobalt and copper leaching rates were 81.54% and 85.48%, respectively.
According to information, the cobalt in gold concentrate is mainly found in cobalt-arsenic or cobalt-like crystal impurities in cobalt-bearing arsenopyrite, and it is necessary to achieve comprehensive recovery of gold, silver, copper and cobalt in gold concentrates. Arsenic in gold concentrates must first be removed. Therefore, on the basis of the two-stage roasting process for arsenic removal, a comprehensive recovery process for gold, silver, copper and cobalt was developed. The process flow is: Stage I roasting, decomposing and calcining at a roasting temperature of 400-500 DEG C, so that arsenic is volatilized and removed by As2O3 gas. Stage II roasting is sulfidation roasting. A certain amount of additives are added for roasting at a roasting temperature of 600 to 650 DEG C. to form arsenate, and arsenate is formed from arsenic, and sulfate is formed from copper and cobalt, which is leached with hot water and dilute sulfuric acid. Arsenic, copper, and cobalt enter the solution and are separated from Au and Ag. Then, from the acid leaching residue, cyanide leaching of Au and Ag, and recovering copper and cobalt from the acid leaching solution, the objective of comprehensive recovery of Au, Ag, Cu, and Co is achieved.
element Au* Ag* Cu Pb Zn Fe S As Co C
content(%) 92.40 40.8 3.10 0.09 0.22 24.58 12.88 18.44 0.65 3.2
Two-stage roasting was used to pretreat the ore sample and then cyanide leaching. The roasting conditions are as follows: Stage I roasting arsenic, roasting temperature 400-500°C, time 40 min; Stage II roasting sulfur removal, roasting temperature 600-650°C, time 30 min, roasting slag using sulfuric acid solution to immerse copper and cobalt. : Sulfuric acid concentration 10%, liquid-solid ratio 4:1, temperature 70-80°C, time 2h. After solid-liquid separation, the leachate remains and Cu and Co are recovered therefrom. The leach residue is subjected to cyanide leaching of Au and Ag. The leaching conditions were as follows: NaCN concentration 0.2%, liquid to solid ratio 2:1, leachate pH ≈9.5 (adjusted with NaHCO3+NaOH), leaching time 36 h. The cyanide leaching test results are shown in Table 2.
element Au Ag Cu* Co*
The original ore grade (1×10-6) 92.40 40.8 3.10 0.65
Cyanide grade (1×10-6) 13.33 32.8 0.65 0.30
Leaching rate (%) 85.57 19.60 79.00 53.85
In order to improve the leaching rate of Au and Ag by two-stage roasting cyanidation and to improve the arsenic removal effect in two stages of roasting, R-reagent was selected as the additive for two-stage calcination cyanide leaching experiment. The conditions are as follows: Stage I decomposition and calcination, temperature 400-500°C, time 40 min, Stage II plus additives (R1, R2, R3) roasting, temperature 600°C-650°C, time 30min, additive amount 10%, calcined slag The leaching was performed with hot water and 10% H2SO4 in sequence, the liquid to solid ratio was 4:1, the leaching temperature was 70-80° C., and the time was 2 h. The hot water and the 10% H2SO4 leaching solution were combined, and Cu and Co in the leaching solution were recovered therefrom. The test results are shown in Table 3.

Composite Drainage Net


HDPE Three dimensional composites drainage net is a new type of drainage geotextile material. It is one three-dimension geonet composited with two needle-punched non-woven geotextiles. Three dimensional composites drainage network consists of a tri-dimension thick vertical rib, and a inclined rip on the top and bottom. Double sided adhesive seepage geotextiles form a"filtration - drainage - ventilation - ." overall performance, and can replace the traditional sand and gravel.wildly used in erosion control, foundation wall drainage, landfill leakage collection, leakage detection, methane gas collection,pond leak detection, roadway and pavement drainage and other subsurface drainage system applications.


Property Unit NLDG
50/D200
NLDG
63/D200
NLDG
70/D200
NLDG
80/D200
NLDG
90/D200
Test
Standard
Drainage Net Specification
Hydraulic conductivity (MD) m2/s 2.8×10-3 2.8×10-3 3.2×10-3 4.0×10-3 5 x10-3 ASTM D4716
Puncture Resistance KN/m 0.17 0.17 0.17 0.17 0.17 ASTM D7005
Core Material Geonet Specification
Thickness mm 5 6.3 7 8 9 ASTM D5199
Density g/cm-3 0.94 0.94 0.94 0.94 0.94 ASTM D1505
Carbon Black Content % 2 2 2 2 2 ASTM D1603
Tensile strength (MD) kN/m 8 10 12 14 16 ASTM D7199
Hydraulic conductivity (MD) m2/s 6 8 10 12 14 ASTM D4716
Geotextile Specification
Unit weight g/m2 200 200 200 200 200 /
Geotextile type Continuous filament non-woven geotextile


Feature&Application
Fatures: Application:
1.Keep long time stable water conductivity.
2.High tensile strength and shearing strength.
3.Anti-corrosion, anti-acid and long service life.
4.It can bear compression loading over 2000 KPa.
5. Excellent drainage function and long time high press loading.
6. Construction convenient, shorten the construction period and reduce costs.
1. Tunnel drainage.
2. Landfill drainage.
3. Railway drainage.
4. Retaining walls drainage.
5. Highway roadbed drainage.
6. Underground structure drainage.
7. Garden and playground drainage.

Company Information

Company Information _____________________

Name:

Shandong Jinruixiang geotextile material Co.,Ltd

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No.,10 Yuansan road High-tech development Zone, Laiwu City.

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Takes R&D as center, innovation as driving force, market as orientation, and talents as foundation.

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Enterprise of Abiding by Strictly Contract and Being Trustworthy

ISO9001:2008 Quality Management System Certification; National Industrial Production License.

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Packing Detail:

Three dimensional composites drainage network rolls can be packaged with woven bags.

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Q : Are you a factory or trading company?

A : We are a professional manufacturer that specialized in geomembrane, geotextile, Composite Geomembrane etc with ISO9001 certificate more than 15 years.

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A : Our facoty is located is No.10 Yuanshan Road High-tech Development Zone, Laiwu District, Jinan City China. You can take the plan to Jinan Yaoqiang International Airport, then we can pick you up.

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A : Yes, we'd love to send a free sample to you for an evaluation if you need.

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Dam Liner,Pond Liner,Composite Drainage Net,Hdpe Geomembrane Dam Liner

Shandong Jinruixiang Geotextile Material Co., Ltd , https://www.jrxgeosynthetics.com